Sodium Bicarbonate → HCID 23683782, compound

HRID 2163392Notes

Reaction equation

HRID 2163392 reaction equation
C(=O)([O-])O.[Na+:5].[O:6]=[C:7]1[C:12]2[CH:13]=[CH:14][C:15]([O:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][O:25][C:26]3[CH:31]=[CH:30][CH:29]=[CH:28][C:27]=3[CH2:32][CH2:33][CH3:34])=[CH:16][C:11]=2[O:10][C:9]([C:35]([OH:37])=[O:36])=[CH:8]1>O>[O:6]=[C:7]1[C:12]2[CH:13]=[CH:14][C:15]([O:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][O:25][C:26]3[CH:31]=[CH:30][CH:29]=[CH:28][C:27]=3[CH2:32][CH2:33][CH3:34])=[CH:16][C:11]=2[O:10][C:9]([C:35]([O-:37])=[O:36])=[CH:8]1.[Na+:5]

Participants

4

Reactant 2

HCID 516892Sodium BicarbonateHCID 13090986HCID 13090986, compound

Product 1

HCID 23683782HCID 23683782, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent2×

Procedure

A solution of 0.412 parts of sodium hydrogen carbonate in 20 parts of water was added to a suspension of 2.19 parts of 4-oxo-7-[7-(2-n-propyl phenoxy)heptyloxy]-4H-1-benzopyran-2-carboxylic acid in 30 parts of water and the mixture heated until a clear solution was obtained. The filtrate was freeze dried to furnish 2.19 parts of sodium 4-oxo-7-[7-(2-n-propyl phenoxy)heptyloxy]-4H-1-benzopyran-2-carboxylate.

Workup

  1. temperaturethe mixture heated until a clear solution
  2. customwas obtained
  3. customdried

Sources & evidence

ORD record
ord-faefbbec6dde4ce091bbbe96284179f6
Source dataset
uspto-grants-1979_01
Patent number
US04133889

Reaction notes

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