HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 22752003, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | HCID 22752000 | HCID 22752000 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 22752003 | HCID 22752003 | — |
Reaction Steps
A solution of 1.4 g of 2,5-diethyl-4-benzylthio-2,3-dihydrofuran-3-one in 50 ml anhydrous ether was treated with 0.88 g of sodium in liquid ammonia as described in Example A7. After working up the reaction mixture the title compound could be isolated by preparative gaschromatography. Relative retention time as compared with 43.1 minutes for dodecane was 51.9 minutes.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04134901 |
| Source dataset | uspto-grants-1979_01 |
| ORD ID | ord-504a746d915746879ac9f0e2fd0f86fa |
| Source note | uspto-grants-1979_01 |