Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2163525Generated: November 4, 2026

1-Bromo-3-chloropropane → HCID 22752785, compound

https://huagongshe.com/reaction/2163525

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1-Bromo-3-chloropropaneHCID 8006—
Reactant6,7-Dimethoxy-4-methyl-1(2H)-phthalazinoneHCID 13327030—
ReactantChloroform methanolHCID 21584188—
SolventDimethylformamideHCID 6228—
ProductHCID 22752785HCID 22752785—

Reaction Steps

1-[4-Methyl-6,7-dimethoxy-1(2H)-phthalazinone-2-yl]-3-chloropropane was prepared analogous to Example 1 (a) by reaction of 4-methyl-6,7-dimethoxy-1(2H)-phthalazinone with 1-bromo-3-chloro-propane in dimethylformamide. Rf -value (chloroform/methanol = 9/1) : 0.9.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04134980
Source datasetuspto-grants-1979_01
ORD IDord-0b3a432b5db243c08b099a70da56c940
Source noteuspto-grants-1979_01