HRID2163525

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID8006

1-Bromo-3-chloropropane

C3H6BrCl

HCID13327030

6,7-Dimethoxy-4-methyl-1(2H)-phthalazinone

C11H12N2O3

HCID21584188

Chloroform methanol

C2H5Cl3O

PRODUCTS

生成物

HCID22752785

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

PROCEDURE

实验过程

1-[4-Methyl-6,7-dimethoxy-1(2H)-phthalazinone-2-yl]-3-chloropropane was prepared analogous to Example 1 (a) by reaction of 4-methyl-6,7-dimethoxy-1(2H)-phthalazinone with 1-bromo-3-chloro-propane in dimethylformamide. Rf -value (chloroform/methanol = 9/1) : 0.9.