HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl-[2-(3,4-dimethoxy-phenyl)-ethyl]-amine → HCID 22752795, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl-[2-(3,4-dimethoxy-phenyl)-ethyl]-amine | HCID 200274 | — |
| Reactant | Chloroform methanol | HCID 21584188 | — |
| Reactant | HCID 22752785 | HCID 22752785 | — |
| Solvent | Chlorobenzene | HCID 7964 | — |
| Product | HCID 22752795 | HCID 22752795 | — |
Reaction Steps
1-[4-Methyl-6,7-dimethoxy-1(2H)-phthalazinone-2-yl]-3-[N-benzyl-N-(2-(3,4-dimethoxy-phenyl)-ethyl)-amino]propane was prepared analogous to Example 1 (a) by reaction of 1-[4-methyl-6,7-dimethoxy-1(2H)-phthalazinone-2-yl]-3-chloro-propane with N-(3,4-dimethoxy-phenylethyl)-N-benzylamine in chlorobenzene. Rf -value (chloroform/methanol = 9/1) : 0.9.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04134980 |
| Source dataset | uspto-grants-1979_01 |
| ORD ID | ord-77b6007982e24dbf8be905ca590c24d7 |
| Source note | uspto-grants-1979_01 |