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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2163532Generated: November 1, 2026

1-Bromo-3-chloropropane → HCID 22752790, compound

https://huagongshe.com/reaction/2163532

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1-Bromo-3-chloropropaneHCID 8006—
ReactantChloroform methanolHCID 21584188—
ReactantHCID 22752805HCID 22752805—
SolventDimethylformamideHCID 6228—
ProductHCID 22752790HCID 22752790—

Reaction Steps

1-[4-Methyl-6,7-ethylenedioxy-1(2H)-phthalazinone-2-yl]-3-chloro-propane was prepared analogous to Example 1 (a) by reaction of 4-methyl-6,7-ethylenedioxy-1(2H)-phthalazinone with 1-bromo-3-chloro-propane in dimethylformamide. Rf -value (chloroform/methanol = 19/1) : 0.9.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04134980
Source datasetuspto-grants-1979_01
ORD IDord-58d6754e101a4c689b8fa2b5a21ecb90
Source noteuspto-grants-1979_01