HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Methylhomoveratrylamine → HCID 12512897, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Methylhomoveratrylamine | HCID 77039 | — |
| Reactant | Chloroform methanol | HCID 21584188 | — |
| Reactant | HCID 22752790 | HCID 22752790 | — |
| Solvent | Chlorobenzene | HCID 7964 | — |
| Product | HCID 12512897 | HCID 12512897 | — |
Reaction Steps
1-4-Methyl-6,7-ethylenedioxy-1(2H)-phthalazinone-2-yl]-3-[N-methyl-N-(2-(3,4-dimethoxy-phenyl)-ethyl)-amino]-propane was prepared analogous to Example 1 (b) by reaction of 1-[4-methyl-6,7-ethylenedioxy-1(2H)-phthalazinone-2-yl]-3-chloro-propane with N-(3,4-dimethoxy-phenylethyl)-N-methyl-amine in chlorobenzene. Yellow oil. Rf -value (chloroform/methanol = 9/1) : 0.7.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04134980 |
| Source dataset | uspto-grants-1979_01 |
| ORD ID | ord-9177574aefa443b6b324471ce5e3e42e |
| Source note | uspto-grants-1979_01 |