Chloroacetyl chloride → HCID 737111, compound

HRID 2163541Notes

Reaction equation

[Cl:1][CH2:2][C:3](Cl)=[O:4].[OH:6][C:7]12[CH2:16][CH:11]3[CH2:12][CH:13]([CH2:15][CH:9]([CH2:10]3)[CH2:8]1)[CH2:14]2>>[Cl:1][CH2:2][C:3]([O:6][C:7]12[CH2:8][CH:9]3[CH2:15][CH:13]([CH2:12][CH:11]([CH2:10]3)[CH2:16]1)[CH2:14]2)=[O:4]

Participants

Reactant 2

HCID 6577Chloroacetyl chloride

HCID 641521-Adamantanol

Product 1

HCID 737111HCID 737111, compound

Procedure

A mixture of 24.8 g (0.22 mol) of chloroacetyl chloride and 30.4 g (0.2 mol) of 1-hydroxyadamantane is heated in an oil bath at 50°-60° until a solution is obtained.

Workup

temperatureis heated in an oil bath at 50°-60° until a solution
customis obtained

Sources & evidence

ORD record: ord-a0eacd88a5b046d4beda2256b8ed8491
Source dataset: uspto-grants-1979_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04134991

Reaction notes

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