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HRID2163583

反应详情

EQUATION

反应方程式

HRID 2163583 的结构方程式

REACTANTS

反应物

1
结构：N#CC(=Cc1cc(Cl)ccc1[N+](=O)[O-])C(N)=O
HCID54133839

未命名化合物

PRODUCTS

生成物

1
结构：NC(=O)c1cc2cc(Cl)ccc2nc1N
HCID12594648

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：[Fe]
催化剂HCID23925

Iron

Fe

PROCEDURE

实验过程

Following the procedure of Example IV-B, α-cyano-β-(2-nitro-5-chlorophenyl)acrylamide (51.0 g., 0.2mole) is treated with iron powder (56 g., 1.0 mole) to provide 19 g. (43%) of the title carboxamide derivative M.P. 250°-251° C. when recrystallized from ethanol.

WORKUP

后处理

  1. customto provide 19 g
  2. custom(43%) of the title carboxamide derivative M.P. 250°-251° C. when recrystallized from ethanol