HRID2163615

反应详情

EQUATION

反应方程式

HRID 2163615 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

To a solution of 1.61g of copper(II) nitrate trihydrate and 1.25g of sodium acetate in 25 ml of deionized water is added a warm solution of 2.08g of 5-chlorosalicylaldehyde in 25 ml of 95% ethanol. The mixture is stirred at 45°-50° C for 15 minutes, cooled, and filtered. The yellow-green solid which results, Bis(5-chlorosalicylaldehyde) copper(II), is rinsed with water and 95% ethanol and dried in vacuo.

WORKUP

后处理

  1. temperaturecooled
  2. filtrationfiltered
  3. customThe yellow-green solid which results
  4. washBis(5-chlorosalicylaldehyde) copper(II), is rinsed with water and 95% ethanol
  5. customdried in vacuo