HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Chloro-salicylaldehyde → HCID 86736250, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Chloro-salicylaldehyde | HCID 12481 | — |
| Reactant | Sodium Acetate | HCID 517045 | — |
| Reactant | Copper(II) nitrate trihydrate | HCID 9837674 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 86736250 | HCID 86736250 | — |
Reaction Steps
To a solution of 1.61g of copper(II) nitrate trihydrate and 1.25g of sodium acetate in 25 ml of deionized water is added a warm solution of 2.08g of 5-chlorosalicylaldehyde in 25 ml of 95% ethanol. The mixture is stirred at 45°-50° C for 15 minutes, cooled, and filtered. The yellow-green solid which results, Bis(5-chlorosalicylaldehyde) copper(II), is rinsed with water and 95% ethanol and dried in vacuo.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04136097 |
| Source dataset | uspto-grants-1979_01 |
| ORD ID | ord-7cc3a7f483c144ea92fc5ba23a547935 |
| Source note | uspto-grants-1979_01 |