Sodium → HCID 74086374, compound

HRID 2163683Notes

Reaction equation

HRID 2163683 reaction equation
S(O)(O)(=O)=O.C1O[C:17]2[CH:16]=[CH:15][C:10]([CH2:11][CH2:12]NN)=[CH:9][C:8]=2O1.[Na].C1OC2C=CC(C[CH2:26][NH:27][N:28]=[C:29]([CH3:33])[C:30]([O-:32])=[O:31])=CC=2O1.[Na+:38]>>[C:10]1([CH2:11][CH2:12][CH2:26][NH:27][N:28]=[C:29]([CH3:33])[C:30]([O-:32])=[O:31])[CH:9]=[CH:8][CH:17]=[CH:16][CH:15]=1.[Na+:38]

Participants

4

Reactant 3

HCID 5360545SodiumHCID 22751343HCID 22751343, compoundHCID 74088064HCID 74088064, compound

Product 1

HCID 74086374HCID 74086374, compound

Procedure

3,4-methylenedioxy-phenethylhydrazine sulphate (m.p. 138°-140° C. (decomp.)) and subsequent preparation of the sodium salt: sodium 2-(3,4-methylenedioxy-phenethylhydrazono)-propionate; m.p. 175°-177° C. (decomp.), after recrystallization from ethanol.

Workup

  1. customm.p. 175°-177° C. (decomp.), after recrystallization from ethanol

Sources & evidence

ORD record
ord-d4030e0ebde045679e30bc1519ec6c10
Source dataset
uspto-grants-1979_01
Patent number
US04136196

Reaction notes

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