Alpha-Methylstyrene → HCID 53915954, compound

HRID 2163692Notes

Reaction equation

HRID 2163692 reaction equation
[C:1]1([C:7]([CH3:9])=[CH2:8])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[S:10](Cl)([Cl:13])(=[O:12])=[O:11]>CN(C)C=O>[C:1]1([C:7]([CH3:9])=[CH:8][S:10]([Cl:13])(=[O:12])=[O:11])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

Participants

4

Reactant 2

HCID 7407Alpha-MethylstyreneHCID 24648Sulfuryl chloride

Product 1

HCID 53915954HCID 53915954, compound

Reagents, catalysts & solvents 1

HCID 6228DimethylformamideSolvent

Procedure

Following the procedure of Preparation A, 2-phenylpropene is reacted with sulfuryl chloride in N,N-dimethylformamide to give 2-phenylpropene-1-sulfonyl chloride, which is then treated with ammonia to give 2-phenylpropene-1-sulfonamide, m.p. 101-102.5° C.

Sources & evidence

ORD record
ord-4020d0a78df6481aa47741504547698a
Source dataset
uspto-grants-1979_01
Patent number
US04136180

Reaction notes

Loading…