HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-chloro-N-methylacetamide → 2-(5-Hydroxy-7-isopropyl-10,10-dimethyl-1,2,4,10-tetrahydro-9-oxa-3-aza-phenanthren-3-yl)-N-methyl-acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-chloro-N-methylacetamide | HCID 66773 | — |
| Reactant | 10-hydroxy-8-isopropyl-5,5-dimethyl-1,2,3,4-tetrahydro-5H-[1]benzopyrano[4,3-c]pyridine | HCID 20287866 | — |
| Product | 2-(5-Hydroxy-7-isopropyl-10,10-dimethyl-1,2,4,10-tetrahydro-9-oxa-3-aza-phenanthren-3-yl)-N-methyl-acetamide | HCID 21321140 | — |
Reaction Steps
The above-titled compound was prepared by reacting 10-hydroxy-8-isopropyl-5,5-dimethyl-1,2,3,4-tetrahydro-5H-[1]benzopyrano[4,3-c]pyridine with 2-chloro-N-methylacetamide according to the method of Example 1; m.p. 178-190°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04137232 |
| Source dataset | uspto-grants-1979_01 |
| ORD ID | ord-4ada01923a79402ca036129ffe45a1a7 |
| Source note | uspto-grants-1979_01 |