HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl chlorophosphate → 1-[Ethoxy(isothiocyanato)phosphoryl]oxyethane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl chlorophosphate | HCID 13139 | — |
| Reactant | Ammonium thiocyanate | HCID 15666 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | 1-[Ethoxy(isothiocyanato)phosphoryl]oxyethane | HCID 556832 | — |
Reaction Steps
The title compound is prepared by the method of M. Kulka [Canadian Journal of Chemistry, 37, 525(1959)]by allowing diethylphosphorchloridate and ammonium thiocyanate to react in benzene; b.p. 76° C. to 83° C./0.5 Torr; nD25 1.4758.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04137310 |
| Source dataset | uspto-grants-1979_01 |
| ORD ID | ord-f2284818d5d348758694439c049c77c8 |
| Source note | uspto-grants-1979_01 |