HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propyl mercaptan → HCID 20301879, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propyl mercaptan | HCID 7848 | — |
| Reactant | Thiophenol | HCID 7969 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2,5-Dichloro-4-nitroaniline | HCID 23108 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 20301879 | HCID 20301879 | — |
| Product | HCID 20301893 | HCID 20301893 | — |
Reaction Steps
Similarly, 2.5-dichloro-4-nitroaniline is allowed to react with n-propyl mercaptan and thiophenol in dimethylformamide at 100° C. in the presence of potassium carbonate to afford 2-chloro-4-nitro-5-n-propylthioaniline, m.p. 125°-127° C., and 2-chloro-4-nitro-5-phenylthioaniline, m.p. 163°-166° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04137310 |
| Source dataset | uspto-grants-1979_01 |
| ORD ID | ord-0a013e0dc62443778cee55a2c9273107 |
| Source note | uspto-grants-1979_01 |