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HRID2164041

反应详情

EQUATION

反应方程式

HRID 2164041 的结构方程式

REACTANTS

反应物

4
结构：CCCS
HCID7848

1-Propanethiol

C3H8S

结构：Sc1ccccc1
HCID7969

Benzenethiol

C6H6S

结构：O=C([O-])[O-].[K+].[K+]
HCID11430

Potassium Carbonate

CK2O3

结构：Nc1cc(Cl)c([N+](=O)[O-])cc1Cl
HCID23108

2,5-Dichloro-4-nitroaniline

C6H4Cl2N2O2

PRODUCTS

生成物

2
结构：CCCSc1cc(N)c(Cl)cc1[N+](=O)[O-]
HCID20301879

未命名化合物

结构：Nc1cc(Sc2ccccc2)c([N+](=O)[O-])cc1Cl
HCID20301893

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN(C)C=O
溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

PROCEDURE

实验过程

Similarly, 2.5-dichloro-4-nitroaniline is allowed to react with n-propyl mercaptan and thiophenol in dimethylformamide at 100° C. in the presence of potassium carbonate to afford 2-chloro-4-nitro-5-n-propylthioaniline, m.p. 125°-127° C., and 2-chloro-4-nitro-5-phenylthioaniline, m.p. 163°-166° C.