HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromine → HCID 22750135, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromine | HCID 24408 | — |
| Reactant | N-(3-acetylphenyl)-5-methylisoxazole-3-carboxamide | HCID 2555322 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 22750135 | HCID 22750135 | — |
Reaction Steps
A solution of bromine (12.5 g) in chloroform (60 ml) was added to a slurry of 3'-acetyl-5-methyl-3-isoxazolecarboxanilide. 1/4 hydrate (19 g) in chloroform (190 ml). The mixture was stirred for 1/2 hour and diluted with diethyl ether. The product was filtered and dried. Yield 21.0 g = (84%,) m.p. 172°-174°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04137321 |
| Source dataset | uspto-grants-1979_01 |
| ORD ID | ord-1f4f2d4264a44f2a8eb9dfe8a62cbcdd |
| Source note | uspto-grants-1979_01 |