HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21527340, compound → HCID 53668716, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21527340 | HCID 21527340 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 53668716 | HCID 53668716 | — |
Reaction Steps
A mixture of 3.4 g. of [2-(aminocarbonyl)-3-benzyloxyphenylamino]oxoacetic acid ethyl ester and 0.3 g. of 5% Pd on charcoal is hydrogenated until hydrogen uptake ceases. The mixture is filtered through celite; the filtrate is evaporated and the residue is recrystallized to give pure product, m.p. 200°-202° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04137325 |
| Source dataset | uspto-grants-1979_01 |
| ORD ID | ord-65fc44bf19904f07b36c4fde02f56c24 |
| Source note | uspto-grants-1979_01 |