Benzonitrile, 3,5-dinitro- → 3-Amino-5-nitrobenzonitrile
Reaction equation
[N+:1]([C:4]1[CH:5]=[C:6]([CH:9]=[C:10]([N+:12]([O-])=O)[CH:11]=1)[C:7]#[N:8])([O-:3])=[O:2]>[Fe]>[NH2:12][C:10]1[CH:9]=[C:6]([CH:5]=[C:4]([N+:1]([O-:3])=[O:2])[CH:11]=1)[C:7]#[N:8]Participants
3
Reactant 1
Product 1
Reagents, catalysts & solvents 1
Procedure
3-amino-5-nitrobenzonitrile is prepared by iron reduction of 3,5-dinitrobenzonitrile as in example 9, m.p. 168°-170° C.
Sources & evidence
- ORD record
- ord-f81133b0a01248ef9186f33b0d26c97b
- Source dataset
- uspto-grants-1979_01
- Patent number
- US04137325
Reaction notes
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