HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Aminopyridine → HCID 54684958, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Aminopyridine | HCID 10439 | — |
| Reactant | HCID 54684933 | HCID 54684933 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | HCID 54684958 | HCID 54684958 | 72% |
Reaction Steps
5-Ethyl-2,5-dihydro-4-hydroxy-2-methyl-N-(2-pyridyl)-1,2 thiazino[5,6-b]indole-3-carboxamide 1,1-dioxide was prepared analogous to Example 15 from methyl 5-ethyl-2,5-dihydro-4-hydroxy-2-methyl-1,2-thiazino[5,6-b]indole-3-carboxylate-1,1-dioxide and 2-amino-pyridine with a yield of 72% of theory. M.p.: 232° C. (decomposition, from xylene).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04137313 |
| Source dataset | uspto-grants-1979_01 |
| ORD ID | ord-264aa67a99e64daea8c47ea232012093 |
| Source note | uspto-grants-1979_01 |