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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2164096Generated: October 31, 2026

2-Aminopyridine → HCID 54684958, compound

https://huagongshe.com/reaction/2164096

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2-AminopyridineHCID 10439—
ReactantHCID 54684933HCID 54684933—
SolventO-XyleneHCID 7237—
ProductHCID 54684958HCID 5468495872%

Reaction Steps

5-Ethyl-2,5-dihydro-4-hydroxy-2-methyl-N-(2-pyridyl)-1,2 thiazino[5,6-b]indole-3-carboxamide 1,1-dioxide was prepared analogous to Example 15 from methyl 5-ethyl-2,5-dihydro-4-hydroxy-2-methyl-1,2-thiazino[5,6-b]indole-3-carboxylate-1,1-dioxide and 2-amino-pyridine with a yield of 72% of theory. M.p.: 232° C. (decomposition, from xylene).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04137313
Source datasetuspto-grants-1979_01
ORD IDord-264aa67a99e64daea8c47ea232012093
Source noteuspto-grants-1979_01