HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aniline → HCID 54684971, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | HCID 54684933 | HCID 54684933 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | HCID 54684971 | HCID 54684971 | 56% |
Reaction Steps
5-Ethyl-2,5-dihydro-4-hydroxy-2-methyl-N-phenyl-1,2-thiazino-[5,6-b]indole-3-carboxamide-1,1-dioxide was prepared analogous to Example 15 from methyl 5-ethyl-2,5-dihydro-4-hydroxy-2-methyl-1,2-thiazino[5,6-b]indole-3-carboxylate-1,1-dioxide and aniline a yield of 56% of theory. M.p.: 268° C. (decomposition; from xylene).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04137313 |
| Source dataset | uspto-grants-1979_01 |
| ORD ID | ord-6cae755bc8e1494d805b7aabcce285e9 |
| Source note | uspto-grants-1979_01 |