HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-4-methylthiazole → HCID 54684970, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-4-methylthiazole | HCID 74143 | — |
| Reactant | HCID 54684959 | HCID 54684959 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | HCID 54684970 | HCID 54684970 | 67% |
Reaction Steps
2,5-Dihydro-2,5-dimethyl-4-hydroxy-N-(4-methyl-2-thiazolyl)-1,2-thiazino[5,6-b]indole-3-carboxamide-1,1-dioxide was prepared analogous to Example 2 from benzyl 2,5-dihydro-2,5-dimethyl-4-hydroxy-1,2-thiazino[5,6-b]indole-3-carboxylate-1,1-dioxide and 2-amino-4-methyl-thiazole in xylene; M.p.: 270° C. (decomp.); Yield: 67% of theory;
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04137313 |
| Source dataset | uspto-grants-1979_01 |
| ORD ID | ord-257a46ea67a040fbaf6f55581c2d8ac3 |
| Source note | uspto-grants-1979_01 |