HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → HCID 22750291, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | Chlorotrimethylsilane | HCID 6397 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 22750311 | HCID 22750311 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 22750291 | HCID 22750291 | — |
Reaction Steps
From 4.4 g. of 6-[4-(1-pyrrolidinylsulfonyl)phenyl]-1,2-dihydro-2-oxonicotinic acid in 150 ml. of methylene chloride, 1.6 ml. of triethylamine, 1.45 ml. of trimethylsilyl chloride and 1.7 ml. of thionyl chloride, following the procedure of a) above, there is obtained 6-[4-(1-pyrrolidinylsulfonyl)phenyl]-1,2-dihydro-2-oxonicotinyl chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04137408 |
| Source dataset | uspto-grants-1979_01 |
| ORD ID | ord-33dd4b6e3b084da18d4e85c6e0517c42 |
| Source note | uspto-grants-1979_01 |