HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22749738, compound → HCID 22749858, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22749738 | HCID 22749738 | — |
| Reactant | HCID 22749852 | HCID 22749852 | — |
| Reactant | Sodium periodate | HCID 23667635 | — |
| Reactant | HCID 70608037 | HCID 70608037 | — |
| Product | HCID 22749858 | HCID 22749858 | — |
| Product | HCID 22749883 | HCID 22749883 | — |
| Product | HCID 70608252 | HCID 70608252 | — |
| Product | HCID 70608772 | HCID 70608772 | — |
Reaction Steps
Each of 7-methoxy-3,7-dimethyloctyl 4-methylthiophenyl ether, 7-methoxy-3,7-dimethyloct-2-enyl 4-methylthiophenyl ether, 7-ethoxy-3,7-dimethyloctyl 4-methylthiophenyl ether and 7-ethoxy-3,7-dimethyloctyl-2-enyl 4-methylthiophenyl ether is treated with sodium metaperiodate according to the process of Example 6 to yield 7-methoxy-3,7-dimethyloctyl 4-methylsulfinylphenyl ether, 7-methoxy-3,7-dimethyloct-2-enyl 4-methylsulfinylphenyl ether, 7-ethoxy-3,7-dimethyloctyl 4-methylsulfinylphenyl ether and 7-ethoxy-3,7-dimethyloct-2-enyl 4-methylsulfinylphenyl ether, respectively. The corresponding 4-methylsulfonylphenyl ether are prepared using the process of Example 7.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04137273 |
| Source dataset | uspto-grants-1979_01 |
| ORD ID | ord-ce1abcab2a1b4a55ba369e374f64295f |
| Source note | uspto-grants-1979_01 |