HCID 13455393, compound → HCID 13455395, compound

Participants

Reaction Steps

A 10-g portion of 1-(2-chloroquinazoline-4-yl)pyridinium chloride was added to 100 ml of pyridine under a calcium sulfate drying tube, refluxed 11/2 hours, then allowed to stir 3 days. The reaction was filtered and the solid was rinsed with pyridine, then ether, and dried in vacuo giving 10.4 g of 1,1'-(2,4-quinazolinediyl)bis[pyridinium] dichloride (m.p. 156°-162° C.).

Provenance & Evidence