HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorine → HCID 13394256, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorine | HCID 24526 | — |
| Reactant | HCID 14100143 | HCID 14100143 | — |
| Reactant | chloroform methanol HOAc | HCID 21866353 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | HCID 13394256 | HCID 13394256 | 100% |
Reaction Steps
A suspension of 4,5-bis(4-methoxyphenyl)-1H-imidazole (10.0 g, 0.036 mol) in 200 ml of carbon tetrachloride was treated with chlorine until no starting material was evidenced by tlc (chloroform-methanol-acetic acid, 17:1:2). The resulting solid was collected by filtration, washed with carbon tetrachloride, and dried in vacuo to yield 12.5 g (100%) of the title compound, m.p. 129°-132° (dec.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04503065 |
| Source dataset | uspto-grants-1985_03 |
| ORD ID | ord-32d353687a154351a6f5cf6d69ee531b |
| Source note | uspto-grants-1985_03 |