Ammonia → Ethanamine, 2-[(2-methoxyphenyl)thio]-

HRID 2164286Notes

Reaction equation

HRID 2164286 reaction equation
Cl[CH2:2][CH2:3][S:4][C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][C:6]=1[O:11][CH3:12].[NH3:13].Cl>>[CH3:12][O:11][C:6]1[CH:7]=[CH:8][CH:9]=[CH:10][C:5]=1[S:4][CH2:3][CH2:2][NH2:13]

Participants

4

Reactant 3

HCID 222AmmoniaHCID 313Hydrochloric AcidHCID 15014016HCID 15014016, compound

Product 1

HCID 20406129Ethanamine, 2-[(2-methoxyphenyl)thio]-

Procedure

by the reaction of o-(2-chloroethylthio)-anisole in liquid ammonia for 8 hours at 120° C.; oil; b.p. 118°-122° C./0.05 mm.Hg.; hydrochloride m.p. 163°-167° C.;

Sources & evidence

ORD record
ord-569e3714ec5c41f7a6a5a89171163b33
Source dataset
uspto-grants-1985_03
Patent number
US04503067

Reaction notes

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