HRID2164354

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID8471

Triethylamine

C6H15N

结构：CC(c1cc(C(C)(C)C)cc(C(C)(C)C)c1O)c1cc(C(C)(C)C)cc(C(C)(C)C)c1O

HCID118899

Tetrabutyl ethylidenebisphenol

C30H46O2

HCID57353436

(Dichloromethyl)silane

CH4Cl2Si

PRODUCTS

生成物

结构：CC1c2cc(C(C)(C)C)cc(C(C)(C)C)c2O[SiH](C)Oc2c1cc(C(C)(C)C)cc2C(C)(C)C

HCID102330270

未命名化合物

收率 51%

PROCEDURE

实验过程

Utilizing the procedure of Example 1, this compound is prepared from 23.0 grams (0.20 mole) dichloromethylsilane, 87.7 grams (0.20 mole) 2,2'-ethylidene-bis(4,6-di-t-butylphenol) and 40.5 grams (0.40 mole) of triethylamine. Recrystallization twice from acetonitrile-toluene gives 49.0 g (51% yield) of white crystals, mp 189°-194° C.

WORKUP

后处理

customRecrystallization twice from acetonitrile-toluene