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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2164396Generated: October 29, 2026

Hydrazine hydrate (1:1) → HCID 13116742, compound

https://huagongshe.com/reaction/2164396

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrazine hydrate (1:1)HCID 24654—
ReactantHCID 13120582HCID 13120582—
SolventWaterHCID 962—
ProductHCID 13116742HCID 13116742—

Reaction Conditions

Temperature90 °C

Reaction Steps

4.2 g of 4-{5-[2-(1-imidazolyl)-ethyl]-thien-2-yl}-4-oxo-butyric acid are suspended in 10 ml of water, 0.8 g of hydrazine hydrate are added and the mixture is stirred at 90° C. for 2 hours. After the mixture has been cooled, it is extracted with chloroform. The chloroform phase is washed with water, dried over Na2SO4 and concentrated to dryness.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04504479
Source datasetuspto-grants-1985_03
ORD IDord-6f5143f4115943d5a1f1a10a8f8fd129
Source noteuspto-grants-1985_03