HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 20500929, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | HCID 54243487 | HCID 54243487 | — |
| Product | HCID 20500929 | HCID 20500929 | — |
Reaction Steps
A solution of 18 g of the preceding compound (XXXVII) in 200 ml of ~7 N hydrochloric ethanol and 200 ml of ethanol is brought to reflux for 36 hours. Then the solvent is evaporated, the residue is taken up in methylene chloride, washed with a sodium bicarbonate solution, then with water, dried on magnesium sulfate, filtered and the filtrate is evaporated. 15 g of expected compound are obtained in the form of oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04504663 |
| Source dataset | uspto-grants-1985_03 |
| ORD ID | ord-5921a0fde0c142a58c344fd63e478fec |
| Source note | uspto-grants-1985_03 |