3-Chloro-N,N-dimethyl-1-propanamine → HCID 13135882, compound

Participants

Reaction Steps

A mixture consisting of 8.5 gm (0.025 mol) of n-butyl 1-(4-bromophenyl)-5-amino-1H-1,2,3-triazole-4-carboxylate, 100 ml of absolute dimethylformamide and 9.1 gm (0.075 mol) of 1-chloro-3-(N,N-dimethylamino)-propane was reacted and worked up as in Example 1. 1.5. gm of the desired compound were obtained, corresponding to 13% of theory, with a melting point of 158° C.

Provenance & Evidence