HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 77975665, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Dicyclohexylcarbodiimide | HCID 10868 | — |
| Reactant | Alclofenac | HCID 30951 | — |
| Reactant | Alanine, methyl ester, hydrochloride (1:1) | HCID 2756298 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 77975665 | HCID 77975665 | — |
Reaction Steps
A suspension of (DL)-alanine methyl ester hydrochloride (2.8 g) in dry methylene chloride (10 ml) containing dry triethylamine (2.8 ml) was added to a solution of 4-allyloxy-3-chloro-phenylacetic acid (4.3 g) in dry methylene chloride (30 ml). N,N'-dicyclohexyl-carbodiimide (DCC; 4.1 g) was added and the reaction mixture was stirred at room temperature.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04505898 |
| Source dataset | uspto-grants-1985_03 |
| ORD ID | ord-ad3754857c324bae8e35e6484816bc0e |
| Source note | uspto-grants-1985_03 |