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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2164567Generated: October 31, 2026

Triethylamine → HCID 12796234, compound

https://huagongshe.com/reaction/2164567

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTriethylamineHCID 8471—
ReactantDicyclohexylcarbodiimideHCID 10868—
ReactantAlclofenacHCID 30951—
ReactantGlycine ethyl ester, hydrochlorideHCID 2723640—
SolventChloroformHCID 6212—
SolventTetrahydrofuranHCID 8028—
ProductHCID 12796234HCID 12796234—

Reaction Steps

4-Allyloxy-3-chloro-phenylacetic acid (4.3 g) was dissolved in dry tetrahydrofuran (20 ml). To the solution was added glycine ethyl ester hydrochloride (2.85 g) in dry chloroform (30 ml) containing dry triethylamine (2.8 ml). DCC (4.1 g) was added and the reaction mixture was stirred overnight at room temperature.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04505898
Source datasetuspto-grants-1985_03
ORD IDord-24d1807aa75a4ca9a0e17173b42ba950
Source noteuspto-grants-1985_03