Thiophenol → HCID 13088594, compound

Participants

Reaction Steps

27.3 g (0.1 mol) of 4,4-dimethyl-1-(4-fluorophenyl)-2-(1,2,4-triazol-1-yl)-pent-1-en-3-one (E,Z isomer mixture) and 11 g (0.1 mol) of thiophenol were stirred with 100 ml of ethanol at room temperature. After 1 hour, the crystals which had separated out were filtered off and dried. 34.7 g (91% of theory) of 4,4-dimethyl-1-(4-fluorophenyl)-1-phenylthio-2-(1,2,4-triazol-1-yl)-pentan-3-one, of melting point 175° C., were obtained.

Provenance & Evidence