Propylamine → HCID 54358507, compound

HRID 2164763Notes

Reaction equation

HRID 2164763 reaction equation
[NH2:1][C:2]1[C:7]([CH:8]=O)=[N:6][C:5]([Cl:10])=[C:4]([S:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH3:19])[N:3]=1.[CH2:20]([NH2:23])[CH2:21][CH3:22]>>[Cl:10][C:5]1[N:6]=[C:7]([CH:8]=[N:23][CH2:20][CH2:21][CH3:22])[C:2]([NH2:1])=[N:3][C:4]=1[S:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH3:19]

Participants

3

Reactant 2

HCID 7852PropylamineHCID 13389077HCID 13389077, compound

Product 1

HCID 54358507HCID 54358507, compound

Procedure

Following the procedures described above in Example 6, Step B, but employing instead 2-amino-5-chloro-3-formyl-6-(n-octylthio)pyrazine (100 mg; 0.342 mMol) prepared in Example 8, Step A, and n-propylamine (25 mg; 0.342 mMol and 20% excess), the title compound was prepared. Elemental Analysis for C16H27N4SCl

Sources & evidence

ORD record
ord-5d49f8f4ceed4cea85391962d7a90dc9
Source dataset
uspto-grants-1985_03
Patent number
US04507299

Reaction notes

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