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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2164777Generated: October 31, 2026

8-Chloro-6-(2-chlorophenyl)-4H-imidazo(1,5-a)(1,4)-benzodiazepine-3-carboxamide → HCID 20403325, compound

https://huagongshe.com/reaction/2164777

Reaction equation

Participants

RoleNameHCIDCharge
Reactant8-Chloro-6-(2-chlorophenyl)-4H-imidazo(1,5-a)(1,4)-benzodiazepine-3-carboxamideHCID 162997—
ReactantHCID 88126211HCID 88126211—
ProductHCID 20403325HCID 20403325—

Reaction Conditions

Temperature115 °C

Reaction Steps

A mixture of 0.0047 mole 8-chloro-6-(2-chlorophenyl)-4H-imidazo[1,5-a][1,4]benzodiazepine-3-carboxamide and 3 ml of dimethyl acetamide dimethyl acetate was heated in an oil bath at a temperature of about 115° C. After cooling the crystals were collected on a glass filter and washed with dimethyl formamide (DMF) and ether.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04507313
Source datasetuspto-grants-1985_03
ORD IDord-72c1db8645d746fba908c98bdfd3b92a
Source noteuspto-grants-1985_03