HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isatoic Anhydride → 2-amino-N-(3-imidazol-1-ylpropyl)benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isatoic Anhydride | HCID 8359 | — |
| Reactant | 1H-Imidazole-1-propanamine | HCID 78736 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | 2-amino-N-(3-imidazol-1-ylpropyl)benzamide | HCID 2798335 | — |
Reaction Steps
Isatoic anhydride (22.0 g) was added in portions to a stirred solution of 3-imidazol-1-ylpropylamine (17.2 g) in dioxan (100 ml) over a period of 15 minutes. Stirring was continued for 40 minutes before the solution was evaporated in vacuo to give 2-amino-N-(3-imidazol-1-ylpropyl)benzamide as a buff coloured solid, used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04507315 |
| Source dataset | uspto-grants-1985_03 |
| ORD ID | ord-dac112eea72f4d938ba811a09fbdef49 |
| Source note | uspto-grants-1985_03 |