HRID2165
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
To a solution of 3-(4-chlorobenzoyl)propionic acid (20 g) in absolute ethanol (200 ml) was added 5 g of hydrazine monohydrate. A thick solid was formed which dissolved after heating. The resulting solution was refluxed for 3 h, cooled and the solid formed filtered and dried to yield 16 g (80%) of 6-(4-chlorophenyl)-4,5-dihydropyridazinone.
WORKUP
后处理
- customA thick solid was formed which
- dissolutiondissolved
- temperatureafter heating
- temperatureThe resulting solution was refluxed for 3 h
- temperaturecooled
- customthe solid formed
- filtrationfiltered
- customdried