HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formic Acid → HCID 23043601, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formic Acid | HCID 284 | — |
| Reactant | HCID 23043605 | HCID 23043605 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 23043601 | HCID 23043601 | 97.7% |
Reaction Steps
The 4-[2-(3,4-dibenzyloxyphenyl)ethyl]benzenamine (4.5 g, 11 mmole) is dissolved in toluene (75 ml) containing formic acid (0.51 g, 11 mmole) and refluxed for two hours. The reaction mixture is evaporated to dryness, and the residue is recrystallized from toluene to afford 4.7 g (97%) of N-formyl-4-[2-(3,4-dibenyloxyphenyl)ethyl]benzeneamine, mp 119°-122° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04939133 |
| Source dataset | uspto-grants-1990_07 |
| ORD ID | ord-c8d60c26b0a14effa4df9932178e7803 |
| Source note | uspto-grants-1990_07 |