HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(3,4-Dimethoxyphenethyl)aniline → HCID 23043617, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(3,4-Dimethoxyphenethyl)aniline | HCID 14256024 | — |
| Reactant | HCID 23043608 | HCID 23043608 | — |
| Product | HCID 23043617 | HCID 23043617 | 48.5% |
Reaction Steps
The preparation is as described for Example 45 using 2,2,7trimethyl-4H-1,3,2-benzodioxasilin-4-one (2.0 g, 10 mmol) and 4[2-(3,4-dimethoxyphenyl)ethyl]benzenamine (2.5 g, 10 mmol). Recrystallization from methanol/DMF gives the pure product (1.9 g) mp 162°-164° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04939133 |
| Source dataset | uspto-grants-1990_07 |
| ORD ID | ord-3242f786f1614811907d73dded510375 |
| Source note | uspto-grants-1990_07 |