HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2165278Generated: November 2, 2026
Trifluoroacetic acid → HCID 131716455, compound
https://huagongshe.com/reaction/2165278
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 56634376 | HCID 56634376 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 131716455 | HCID 131716455 | — |
Reaction Steps
(3S-trans) -[[3-[(t-Butyloxycarbonyl)amino]-4-methyl-2-oxo-1-azetidinyl]oxy]acetic acid. phenylmethyl ester (3.6g) was dissolved in 5 ml of dichloromethane and the solution was cooled to -10° C. Trifluoroacetic acid (25ml) was added dropwise and the mixture was stirred for 20 minutes at -10° C. After evaporation, the residue was treated with ether yielding 2.5 g of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04939253 |
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| Source dataset | uspto-grants-1990_07 |
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| ORD ID | ord-a40367852c084f3fb2d897c77b1b99c4 |
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| Source note | uspto-grants-1990_07 |
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