HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl propionate → Undec-1-en-1-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl propionate | HCID 11124 | — |
| Reactant | HCID 53793572 | HCID 53793572 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Undec-1-en-1-ol | HCID 44135745 | — |
Reaction Steps
In about the same way as described under Example 2, an experiment was carried out with difference being that 10 ml methyl-undecenoate was included in the autoclave instead of 10 ml methylpropionate, while after 5 min hydrogen was added until a pressure increase of 30 bar was reached. The autoclave was kept at 80° C. for 5 hours giving a yield of 2.4 g methanol and about 1 g 1-undecenol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04939307 |
| Source dataset | uspto-grants-1990_07 |
| ORD ID | ord-c7a6d286cf5845f1924c8c7357de989a |
| Source note | uspto-grants-1990_07 |