HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Allylphenol → o-Allylphenol 1,3-bisglycidylresorcinol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Allylphenol | HCID 15624 | — |
| Reactant | Lactate | HCID 91435 | — |
| Reactant | 1,3-Bisglycidylresorcinol | HCID 23044773 | — |
| Reactant | Triphenylethyl phosphonium iodide | HCID 66760890 | — |
| Product | o-Allylphenol 1,3-bisglycidylresorcinol | HCID 86742605 | — |
Reaction Conditions
| Temperature | 140 °C |
|---|
Reaction Steps
In a similar manner to that described in Example 1, o-allylphenol (134 g), 1,3-bisglycidylresorcinol (115.1 g), triphenylethylphosphonium iodide (0.75 g) and methylglycolate (145 g) were reacted at 100° C. for 13 hours. The solvent and excess o-allylphenol were removed by heating at 140° C. finally in vacuo. The yield of adduct was 227.9 g and it showed a viscocity of 280 mPa.s at 70° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04939305 |
| Source dataset | uspto-grants-1990_07 |
| ORD ID | ord-5486ac1a6a5f4f9fa0f82c7893b69a74 |
| Source note | uspto-grants-1990_07 |