HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 178476703, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Methyl 2,2,2-trichloroacetimidate | HCID 100479 | — |
| Reactant | 3,4-Diaminoquinoline | HCID 1514289 | — |
| Product | HCID 178476703 | HCID 178476703 | 80% |
Reaction Steps
In the same manner as in Ref. Ex. 17, 1.59 g of 3,4 -diaminoquinoline (V-1) in 20 ml of acetic acid was treated with 1.9 g of methyl trichloroacetimidate to give 3.13 g (yield: 80%) of the titled compound (VIII-2).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04940714 |
| Source dataset | uspto-grants-1990_07 |
| ORD ID | ord-ed8cfe6e2faf493caa54512627386ff6 |
| Source note | uspto-grants-1990_07 |