HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Amino-1,1-dimethylthiourea → HCID 136404502, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Amino-1,1-dimethylthiourea | HCID 2733700 | — |
| Reactant | HCID 14210976 | HCID 14210976 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 136404502 | HCID 136404502 | — |
Reaction Steps
A solution of 11.7 g (0.041 mol) of 2-bromo-1-(5-tert.butyl)-3-methyl-4-hydroxyphenyl)-ethanone from step (a) and 4.4 g (0.037 mol) of 4,4-dimethylthiosemicarbazide in 130 ml of ethanol was refluxed briefly. After cooling, the reaction mixture was worked up corresponding to Example 1(b).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04940790 |
| Source dataset | uspto-grants-1990_07 |
| ORD ID | ord-b1e6f046519b49ad90178f2282fbedd0 |
| Source note | uspto-grants-1990_07 |