Hydrochloric Acid → HCID 23042437, compound

HRID 2165794Notes

Reaction equation

HRID 2165794 reaction equation
[CH2:1]([C:13]1[CH:19]=[CH:18][C:16]([NH2:17])=[CH:15][CH:14]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12].[ClH:20]>O>[ClH:20].[CH2:1]([C:13]1[CH:14]=[CH:15][C:16]([NH2:17])=[CH:18][CH:19]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 77014-Dodecylaniline

Product 1

HCID 23042437HCID 23042437, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

100 parts of p-dodecylaniline were added to 500 parts of water. 100 parts of concentrated hydrochloric acid were added to the solution to give p-dodecylaniline hydrochloride solution. The solution was slowly added to a solution of 50 parts of C. I. Solubilized Sulphur Black 1 in 500 parts of boiling water under stirring. A crystallization began immediately. After the completion of the addition of the p-dodecylaniline hydrochloride solution, a spot test was conducted. No coloration was observed in the exudate. The crystal thus formed was separated by filtration, washed with water and dried to give a water-insoluble black pigment of the following formula: ##STR15## It had λmax of 569 nm in N-methylpyrrolidon.

Sources & evidence

ORD record
ord-28f988356767429c9a90ffc3742d850d
Source dataset
uspto-grants-1990_07
Patent number
US04941923

Reaction notes

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