Dichloromethane → HCID 19755541, compound

Participants

Reaction Steps

44 g of 5-nitro-2-chlorobenzenesulfonyl chloride and 100 ml of. dichloromethane were blended, and a dichloromethane solution containing 48.4 g of methyloctadecylamine and 36.1 ml of triethylamine was added dropwise thereto. After completion of the reaction, the reaction solvent was removed by distillation under reduced pressure. 300 ml of methanol was added to the residue and dissolved, and then the resulting solution was gradually cooled to precipitate a crystal. The crystal was taken out by filtration and dried. Yield: 64 g, 74%.

Provenance & Evidence