HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 14209230, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Phenylethanolamine | HCID 1000 | — |
| Reactant | 4,7-Dichloroquinoline | HCID 6866 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Solvent | 1-Ethoxyethanol | HCID 10129898 | — |
| Product | HCID 14209230 | HCID 14209230 | — |
Reaction Steps
A solution of 4,7-dichloroquinoline (19.8 g), 2-amino-1-phenylethanol (13.7 g) and 20 ml of triethylamine (14.5 g) in 10 ml of ethoxyethanol was heated at 130° C. overnight. The mixture was poured into 600 ml of water and the solid product was collected by filtration recrystallized from ethoxyethanol and washed with ethanol. The yield was 16 g, mp 221°-222° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04942168 |
| Source dataset | uspto-grants-1990_07 |
| ORD ID | ord-23bd111840004b6bacf3213ca4800e45 |
| Source note | uspto-grants-1990_07 |