HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Nitrobenzaldehyde → 3,6-Di(p-nitrostyryl)pyridazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Nitrobenzaldehyde | HCID 541 | — |
| Reactant | 3,6-Dimethylpyridazine | HCID 527031 | — |
| Solvent | Acetic Anhydride | HCID 7918 | — |
| Product | 3,6-Di(p-nitrostyryl)pyridazine | HCID 54059565 | 44.4% |
Reaction Steps
First, 24 g of 3,6-dimethylpyridazine and 60 g of p-nitrobenzaldehyde were dissolved in 1 liter of acetic anhydride, then heated under reflux so as to obtain 33 g of 3,6-di(p-nitrostyryl)pyridazine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04945021 |
| Source dataset | uspto-grants-1990_07 |
| ORD ID | ord-170eb1cb39f94645ba5f78a4b33499dd |
| Source note | uspto-grants-1990_07 |